====== Lab Safety ====== [[https://en.unimib.it/about-us/safety-workplace|Università di Milano-Bicocca: Safety]] ===== General Rules of Conduct ===== * never stay alone in the laboratory ((all equipment can be remotely supervised))((Under no circumstances may students remain without supervision)) * carefully read the instruction manuals of the instruments used * before leaving the laboratory, always ensure that all instruments are in safe condition ([[safety:check-list|check-list]]) * use helmets, gloves, and protective goggles when necessary * record all operations performed in the appropriate logbooks * mark hazardous areas with the red-and-white chain or tape * if it is necessary to access the laboratory outside the department's opening hours, two people must be present and the Supervisor must be informed in advance * do not tamper with or remove safety devices * keep clear access to the black doors that serve as the laboratory's emergency exits (do not block corridors or doors, …) * keep clear access to laboratory doors * do not remove mezzanine railings * wear suitable shoes (for example closed and without heels) to prevent accidents on stairs and protect against impacts or small accidental spills of cryogenic liquids ===== Reference Persons ===== * {{:sicurezza:sinottico_obblighi_responsabili.pdf|Supervisor (document in italian)}} for research and teaching activities: Marco Faverzani (tel. 2225) * In the absence of the supervisor, the most experienced person is responsible for laboratory activities: normally Elena Ferri (tel. 2354) * Head of Prevention and Protection Service (RSPP), University of Milano-Bicocca: Francesca Peltrera (tel. 6109) (email [servizio.prevenzione@unimib.it](mailto:servizio.prevenzione@unimib.it)] * Head of [[https://www.mib.infn.it/main/pages/servizi/prevenzione-e-protezione.php|Prevention and Protection Service (RSPP)]] (INFN Milano-Bicocca Section): Giuseppe Bestiani (tel. 2330) * Qualified Expert, Department of Physics: Stefano Giunti (external); for issues related to radioprotection, contact Marco Faverzani * Cryogenic liquids manager: Roberto Gaigher (tel. 2312) * Personnel authorized to use lifting equipment: Giancarlo Ceruti, Angelo Nucciotti ===== Emergencies ===== * [color=red]accident/injury[/color]: reception (2099) and 112 * [color=red]large fire[/color]: reception (2099) and 112 (make sure the fire alarm has been triggered) * ALWAYS FOR ANY EMERGENCY: reception (2099) * [[[https://www.unimib.it/ateneo/sicurezza-ateneo/caso-emergenza|University](https://www.unimib.it/ateneo/sicurezza-ateneo/caso-emergenza|University) Emergency Page]] * [[https://en.unimib.it/about-us/health-and-safety/emergency-procedures|University Emergency Page]] * {{ :sicurezza:mod108_infoemergenze.pdf |Practical Guide in Case of Emergency (document in italian)}} * For maintenance requests contact Marco Faverzani or Elena Ferri * {{ :sicurezza:pop_8.2_03_pianoemergenza_ed_evacuazione_20190118.pdf |University Emergency and Evacuation Plan (document in italian)}} * {{:sicurezza:addetti2014del04072014.xlsx|List of emergency and first-aid personnel TO BE UPDATED}} * {{:sicurezza:procedure_di_emregenza_edificio_u2.pdf|U2 Building Emergency Procedures for External Operators (document in italian)}} * {{:sicurezza:u2piano_-3.pdf|Evacuation Plan -3}} ===== In Case of Oxygen Deficiency Alarm ===== * leave the laboratory immediately * immediately report the alarm to the supervisor * do not disable the alarm * in any case, do not re-enter the laboratory until the external display shows that oxygen levels have returned to normal (>20%) and until the visual alarm outside the lab has been turned off * do not tamper with safety systems: * do not bypass the solenoid valve that intercepts the gaseous nitrogen line * do not damage oxygen sensor capsules by exposing them to solvent vapors or gas flows * immediately report any anomalies in the oxygen sensors to the supervisor ===== In Case of Blackout ===== * in case of blackout, the [[http://172.17.47.144/|UPS]] (Uninterruptible Power Supply) system, thanks to its battery backup, will ensure the operation of cryostats, oxygen sensors, certain lights, and other equipment connected to panels with a red label until the batteries are depleted (actual duration depends on total load) * computers connected to the UPS will automatically shut down after a few minutes * in case of blackout, the air conditioning and ventilation system (([[http://artico.mib.infn.it/cgi-bin/utareport_html|Status of the Air Treatment Unit, UTA (accessible only from the mib.infn.it domain)]])) stops immediately * once UPS backup ends, the oxygen monitoring system will no longer be active * in case of a prolonged blackout, if necessary, use the UPS time to safely secure cryogenic systems and leave the laboratory; otherwise, leave immediately * in any case, once UPS backup ends, leave the laboratory immediately ===== Regulations ===== * Workplace Safety ((students, undergraduates, PhD students, and research fellows are considered full workers)) - {{ :sicurezza:d.lgs._626-94.pdf |Legislative Decree 626 of 1994 (document in italian)}} - {{ :sicurezza:d.m.363del1998.pdf |Ministerial Decree 363 of 1998 (document in italian)}} - {{ :sicurezza:regolamento.pdf |Regulation for Implementation of DM 363/1998 in Bicocca (document in italian)}} - {{ :sicurezza:d_lgs_230-95.pdf |Legislative Decree 230 of 1995 (document in italian)}} - {{ :sicurezza:dlgs81.pdf |Legislative Decree 81 of 2008 (Workplace Safety) (document in italian)}} - {{ :sicurezza:20200812_201_so_029.pdf |Legislative Decree 101 of 2020 (Radiation Protection) (document in italian)}} ===== Cryogenic Liquids ===== * Liquids used in the laboratory * Liquid helium (T=4K) * Liquid nitrogen (T=77K) * risk of cold burn * always use cryogenic gloves * wear protective goggles * do not touch cold parts with bare hands (especially metals) * risk of asphyxiation ((the volume change from liquid to gas is about 700 times: 1 liter becomes 0.7 m³)) * pay attention to oxygen sensors: in case of alarm, leave the laboratory immediately and report the risk * keep liquid helium containers connected to the copper recovery line * risk of explosion ((the volume change from liquid to gas is about 700 times: 1 liter becomes 0.7 m³)) * check the opening of safety valves * check the closure of vent valves * always check pressure difference before opening a valve * keep all containers vertical * do not use dewars to pour liquid * always close containers with proper lids * beware of ice plugs formation (possible high pressure) * in doubt, call the responsible person * {{ :sicurezza:safety_weisand.pdf |Safety chapter extracted from "Handbook of Cryogenic Engineering", J. Weisand}} * {{ :sicurezza:inventario_liquidi_criogenici_lab-3.xls |Inventory of cryogenic liquids and evaluation of evaporation impact}} * {{ :sicurezza:azoto_refrigerato_2004.pdf |Liquid Nitrogen Safety Data Sheet (document in italian)}} * {{ :sicurezza:elio_liquido.pdf |Liquid Helium Safety Data Sheet (document in italian)}} ===== Pressurized Gases ===== * gases distributed in the laboratory: compressed air, nitrogen, and helium * high pressures may also occur in dilution refrigerator circuits * always close both valves at the take-off points * before opening valves, set the regulators to minimum * keep regulators below 500 mbar * use suitable hoses for gas withdrawal and always check their condition before use * do not tamper with safety valves * always check pressure difference before opening a valve ===== Radioactive Sources ===== * Students are not authorized to handle radioactive sources * Do not touch with bare hands * Do not touch the active part * Keep at a safe distance from body and hands * Protect eyes * Limit exposure time * Handle with tongs * Always clearly label sources (indicating type and activity) * Store unused sources behind lead shielding * Study documentation before use * Sources used in the laboratory: - {{ :sicurezza:co60-handbookrad.pdf |60Co}} - {{ :sicurezza:handbookrad-fe55.pdf |55Fe}} - {{ :sicurezza:handbookrad-na22.pdf |22Na}} - {{ :sicurezza:handbookrad-cd109.pdf |109Cd}} - {{ :sicurezza:handbookrad-co57.pdf |57Co}} - {{ :sicurezza:handbookrad-am241.pdf |241Am}} ===== Lifting Equipment ===== * overhead crane, electric hoist, forklift, and pallet truck may only be used with support from authorized personnel * when working with suspended loads, wear protective helmets ===== Electrical System ===== * it is strictly forbidden to tamper with electrical systems * access to electrical panels is allowed only for maintenance staff * it is strictly forbidden to tamper with electrical connections of instrumentation * do not leave computers or control panels open * electrical connections of equipment must only be made by electricians * do not overload power strips; always check the maximum rating * do not connect multiple power strips in series * do not leave power strips on the floor, especially near areas where cryogenic liquids are used ===== Procedures ===== * [color=red]New Safety Procedures for UNIMIB Research Laboratories (10/02/2023)[/color] [[https://www.unimib.it/ateneo/sicurezza-ateneo/modulistica-e-procedure|Forms and procedures (website in italian)]] * General operating procedures provided by the Prevention and Protection Service * {{:sicurezza:poplab001en-it.pdf|poplab001en-it.pdf}} * {{:sicurezza:poplab002aspec.pdf|poplab002aspec.pdf (document in italian)}} * {{:sicurezza:poplab005.pdf|}} * {{:sicurezza:poplab012_utilizzo_gas.pdf|poplab012_utilizzo_gas.pdf (document in italian)}} * Complete documentation {{:sicurezza:procedure_applicabili_lab_criostati.zip|}}{{:sicurezza:moduli.zip|}} * [[safety:procedures|here]] you can find specific procedures for all operations involving various risks * Each laboratory user must review * all general Operating Procedures listed above * the specific rules, instructions, and procedures for the Cryostats laboratory available on this page or through links * Each laboratory user must sign {{:sicurezza:mod052_ricevuta_di_consegna_materiale_informativo_per_sicurezza_e_salute_.pdf|Form 052}} (Acknowledgment of receipt of safety and health information) * Each laboratory user must print and sign this page ===== Bibliography (must read!) ===== * {{:sicurezza:safety_matters_usc0001.pdf|"Safety Matters", Oxford Instruments}} * {{:sicurezza:practical_cryogenics.pdf|"Practical Cryogenics", Oxford Instruments}} --- \ \ The undersigned ......................................................................... declares to have **read and understood** the information contained in this page, in the attached documents, and in the linked pages. Date .............................................. Signature .............................................